I wouldn't assume they're done, though. You may have more go off, so be careful.
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I have volume increments labeled on all of my carboys. I think that the volume is accurate.
I have wondered if I over-carbonate, and reduce the pressure, will the CO2 move from my keg into my gas tank?the answer to this is a definite no. at 21c [69f] the pressure in your co2 tank will be about 838psi. standard corny kegs are rated to only 130psi, so you'd have keg all over your face long before you got co2 back in the tank.
Why would this produce more sediment?
does that work for any size starter? would you get about the same amount from 100mls from a 2L starter and a 4L starter?