I tried boiling DME in a flask once. It didn’t go so well. ...as in volcanic eruption. I’ve used a stainless pot ever since.
Sent from my iPad using Tapatalk
Ah, yeah. If you're boiling in a flask and don't want the science fair volcano demonstration, you need to use antifoam like Fermcap. It's because the small opening has the same effect as leaving a lid on your pot, guaranteed boil over. A couple of drops of Fermcap, and you can put your foil on top, your stir bar (gasp!) in the flask, and let the boil sanitize everything. Without Fermcap, do not attempt boiling in a flask. Unless you really find a burnt sugar finish attractive on your stovetop.
Note to Rob: It was really good to see you yesterday. We need to get together sometime, maybe at one of the Akron breweries, and chew the fat some more!
With regard to boiling in a flask, I add the DME and a very small amount of yeast nutrient when the water gets hot, but not quite boiling, top it up to the correct volume calculated for the starter, and bring it to a slow boil. Yes, the mixture will tend to foam up when boiling. When I see that starting to happen, I simply remove the flask from the heat source (use a glove to avoid burning your hand), wait a minute or two until the foam drops down, replace it on the burner, and restart the timer. You may have to do this several times until the surface tension on the top of the liquid changes enough to suppress the foam. Boiling with less intense heat will also help. Yes, Fermcap does work, but I never use the stuff as it is silicon based as I can control the risk of boil over pretty well.
One thing I forgot to mention in my original post, invest in a wire gauze to protect the borosilicate glass flask from hot spots from the heat source. Wire gauze is a steel mesh that has a circle of nonflammable material in the center (when I was in college chemistry courses many moons ago, the stuff in the center used to be impregnated with asbestos, but it is now some type of heat resistant ceramic material). Hot spots can weaken the glass over time and the wire gauze spreads the heat evenly over the entire bottom surface of the flask. You can find it at any online scientific supply house. I got mine from Fisher Scientific. They are reasonably priced and a good insurance policy to protect your glassware.
Is my chemistry nerdiness showing again?